TRIFLUOROMETHANESULFONAMIDE Kunye CAS 421-85-2

I-TRIFLUOROMETHANESULFONAMIDE Nge-CAS 421-85-2 Umfanekiso obonakalayo

I-CAS:421-85-2

MF:CH2F3NO2S

MW:149.09

Inombolo ye-EINECS:431-270-1

Izithethantonye:I-Trifluoromethanesulfonamide 96%; trifluoromethylsulfonamide; I-Trifluoromethanesulphonamide 98%; Trifluoromethanesulphonami 98%; I-Trifluoromethanesulfonimidicacid; TrifluoroMethanesulfonaMide 95%; I-TRIFLAMIDE

Shiya uMyalezo Wakho

Iinkcukacha zeMveliso

Khuphela

Iithegi zeMveliso

Yintoni i-TRIFLUOROMETHANESULFONAMIDE Nge-CAS 421-85-2?

I-Trifluoromethanesulfonamide yi-organic intermediate, enokuthi ilungiswe ngokusabela kwe-trifluoromethanesulfonyl chloride kunye negesi ye-ammonia. I-Trifluoromethanesulfonyl ingasetyenziselwa ukulungisa i-LiTFSI. I-LiTFSI yeyona nto ibalaseleyo yokongeza i-electrolyte yeebhetri ze-lithium. Ngenxa yokwakheka kweekhemikhali ezikhethekileyo zecandelo le-anion (CF3SO2) 2N-, i-LiTFSI inozinzo oluphezulu lwe-electrochemical kunye nokuhanjiswa kombane; Xa kuthelekiswa ne-LiClO4 kunye ne-LiPF6, i-LiTFSI njenge-additive electrolyte inokuthi: 1) iphucule ifilimu ye-SEI yee-electrodes ezintle kunye nezibi; 2) ukuzinzisa i-interface ye-electrodes efanelekileyo kunye nembi; 3) inqanda ukuveliswa kwegesi; 4) ukuphucula ukusebenza komjikelo; 5) ukuphucula ukuzinza kweqondo lokushisa eliphezulu; 6) Ukuphucula ukusebenza kokugcinwa kunye nezinye iingenelo.

Inkcazo

Into	Umgangatho
Imbonakalo	Ukuqina kwekristale emhlophe
Isivavanyi	≥98%
Ukufuma	≤0.50%

Isicelo

Yongeza i-172g ye-98% CF3SO2Cl (1mol) kunye ne-500mL ye-acetonitrile ye-anhydrous emva kokunyanga kwamanzi kwi-reactor evaliweyo kunye ne-thermometer, i-stirrer, kunye ne-nitrogen kunye nokususwa kwe-oxygen. Irhasi ye-ammonia okanye isixa esihambelanayo se-ammonium carbonate eyomileyo inyuswa ngokuthe ngcembe kwiqondo lobushushu begumbi phantsi kokuvuselela, kwaye ukusabela kupheliswa emva kweeyure ezi-3 zokusabela. Imveliso ye-ammonium chloride kwisisombululo sokuphendula yasuswa ngokuhluzwa, i-solvent kwi-filtrate yachithwa phantsi koxinzelelo oluncitshisiweyo, kwaye yomiswa phantsi koxinzelelo oluncitshisiweyo kwi-50 ° C ukufumana i-wafer emhlophe ekrwada i-trifluoromethanesulfonamide enesivuno esingekho ngaphantsi kwe 96%.